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APS - 22-ID

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Beamline Name 22-ID
Primary Contact: NameJohn Chrzas
Secondary Contact: NameJohn Rose
Owner/OperatorSER-CAT
Statusoperational
%Time Available (general use)25
ExperimentsMAD
Experiments DetailsMAD, SAD and Microdiffraction
Special CapabilitiesAutomated Sample Screening
Special Capabilities Detailsautomated data reduction and on-site cluster-based structure determination
ServicesRemote access, 6 hr shifts, 19 hr on-stie support
Services DetailsBoth mail-in and remote data collection available to CAT members
Source TypeINSERTION DEVICE
Source DetailsUndulator A
Spot Size (mm): Height0.08
Spot Size (mm): Width0.04
Monochromatordouble crystal - liquid nitrogen cooled
Optics DetailsSi 111. Rosenbaum-Rock double-crystal monochromator: liquid nitrogen cooled; sagitally focusing 2nd crystal, Rosenbaum-Rock vertical focusing mirror
Crystal TypeSi (111)
Mirrorsvertical focusing
Flux(PHOTONS/SEC)7 x 10^12
Flux Detailsfull beam @ 12 keV: 7 x 10(to the 12th power)
Wavelength Range (Å)0.5 - 2.0
Energy Range (keV)6 - 22
GoniometerKappa & single axis phi available
Goniometer DetailsMaatel MD2 microdiffractometer
Sample Handling: Manualpin length (14-22 mm)
Sample Handling: RoboticsModified ALS/Berkeley automounter
Robotics: More InfoThe sample changer has a capacity of 15 pucks, 240 samples (ALS and Unipuck compatible)
Detector: TypeCCD
Detector: ModelMARMOSAIC 300
Detector: Details4 X 4 mosiac
Detector: Activated for Service2005-04-07
Detector: Removed from Service
Removed from Service: DetailsNever
Cryo CapabilityOxford Instruments cryojet
Cryo Capability Details100K
Lab FacilitiesComprehensive wet lab, cold room and crystallization facilities
1. Software: NameSERGUI
1. Software: ClassificationControl/collection
2. Software: NameHKL2000, d*TREK, XGEN, XDS, MOSFLM, PROTEUM2, cmdDENZO, cmdd*TREK, cmdXDS
2. Software: ClassificationProcessing
3. Software: NameSGXPro, SHELXD, ISAS, SOLVE/RESOLVE, PHENIX, CCP4, CNS, EMPR, PHASER, AMORE
3. Software: ClassificationPhasing/refinement
4. Software: NameCOOT, XtalView, Arp/Warp, MAID
4. Software: ClassificationModeling/graphics
HardwareNumerous Linux workstations and a 1.1 TB Linux cluster
Backup Services100 TB PANSAS storage system, Firewire Drives, 10 GB network